HuagongsheHuagongshe Chemistry Print Report · For research reference only
Mesitylene → HCID 69117214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Mesitylene | HCID 7947 | — |
| Reactant | 2'-Allyloxy-2,4-dichloro-6'-fluorobiphenyl | HCID 69117199 | — |
| Product | HCID 69117214 | HCID 69117214 | 65% |
Reaction Steps
A solution of 2′-allyloxy-2,4-dichloro-6′-fluorobiphenyl (1.7 g, 5.7 mmol) in mesitylene (50 mL) was refluxed for 48 h. The solvent was removed under reduced pressure. Purification by ISCO using a solvent gradient of 0 to 20% ethyl acetate in hexanes provided 1.1 g (65%) of 3-allyl-2′,4′-dichloro-6-fluorobiphenyl-2-ol as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365095B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-a484fc6f7c3542d7b1ccaac581aa49dc |
| Source note | uspto-grants-2008_04 |