HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69117214, compound → HCID 69117466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69117214 | HCID 69117214 | — |
| Catalyst | HCID 178424406 | HCID 178424406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69117466 | HCID 69117466 | 73% |
Reaction Steps
Treatment of 3-allyl-2′,4′-dichloro-6-fluorobiphenyl-2-ol (1.1 g, 3.70 mmol) with dichlorobis(acetonitrile)palladium (II) (0.15 g, 0.58 mmol) in methylene chloride (50 mL) according to the procedure described for Example 69, Step 5 provided 0.8 g (73%) of 2′,4′-dichloro-6-fluoro-3-(prop-1-enyl)biphenyl-2-ol as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365095B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-a45c05b199424df8ab38a57f91a41cba |
| Source note | uspto-grants-2008_04 |