HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69117241, compound → HCID 69117474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69117241 | HCID 69117241 | — |
| Catalyst | HCID 178424406 | HCID 178424406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69117474 | HCID 69117474 | 93.2% |
Reaction Steps
Treatment of 3-allyl-5-fluoro-2′-phenylbiphenyl-2-ol (3.0 g, 9.8 mmol) in methylene chloride (100 mL) with dichlorobis(acetonitrile)palladium (II) (0.50 g, 1.93 mmol) according to the procedure described for Example 69, Step 5 provided 2.78 g (93%) of 5-fluoro-2′-phenyl-3-(prop-1-enyl)biphenyl-2-ol as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365095B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-6346184714f444c09e85fb1cebc1ed77 |
| Source note | uspto-grants-2008_04 |