Hydrochloric Acid → HCID 68615345, compound

HRID 902546Notes

Reaction equation

HRID 902546 reaction equation
[Cl:1][C:2]1[C:3]([C:9]2[C:17]3[C:13](=[CH:14][N:15]([CH3:18])[N:16]=3)[CH:12]=[CH:11][CH:10]=2)=[N:4][CH:5]=[C:6]([Cl:8])[CH:7]=1.Cl>CCOCC>[ClH:1].[Cl:1][C:2]1[C:3]([C:9]2[C:17]3[C:13](=[CH:14][N:15]([CH3:18])[N:16]=3)[CH:12]=[CH:11][CH:10]=2)=[N:4][CH:5]=[C:6]([Cl:8])[CH:7]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 597022797-(3,5-Dichloro-2-pyridinyl)-2-methyl-2H-indazole

Product 1

HCID 68615345HCID 68615345, compoundYield 164.2%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

To a solution of 7-(3,5-dichloro-pyridin-2-yl)-2-methyl-2H-indazole (0.042 g) in ether was added a 2 M solution of HCl in ether. The mixture was filtered to afford 0.039 g of 7-(3,5-Dichloro-pyridin-2-yl)-2-methyl-2H-indazole hydrochloride as a yellow solid.

Workup

  1. filtrationThe mixture was filtered

Sources & evidence

ORD record
ord-9c4e185d456d46c580840cd2266b6aff
Source dataset
uspto-grants-2008_04
Patent number
US07365211B2

Reaction notes

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