HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 23122197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-(Prop-2-en-1-yl)oxolan-2-one | HCID 12535140 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 23122197 | HCID 23122197 | — |
Reaction Steps
In an amount of 112 mg of 3-allyldihydrofuran-2-one (WO99/36419) was dissolved in 1 ml of 1,2-dimethoxyethane, added with 1.2 ml of 28% aqueous ammonia, and stirred at room temperature for 17 hours. The reaction mixture was concentrated under reduced pressure to obtain 130 mg of 1-(2-hydroxyethyl)-3-butenecarboxamide. Physicochemical Properties of this Compound
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365174B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-bae905a43cfd4a12b043cc0236658394 |
| Source note | uspto-grants-2008_04 |