HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69252350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10196601 | HCID 10196601 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 69252350 | HCID 69252350 | 99% |
Reaction Steps
To a solution of 2-(3-{3-[[2-chloro-3-(trifluoromethyl)benzyl](2-acetoxy-2-phenyl-ethyl)amino]propoxy}-phenyl)acetic acid in ethyl ether was added HCl in diethyl ether (1.0M). The suspension was filtered and dried to give the title compound as a white solid (99%). NMR(400 MHz, CD3OD) δ: 7.8 (m, 3H), 7.3 (s, 5H), 7.1 (t, J=4.0 Hz, 1H), 6.7 (m, 3H), 6.1 (m, 1H), 4.0 (m, 2H), 3.6-3.4 (m, 7H), 2.2 (m, 2H), 1.9 (s, 3H), 1.1 (t, J=4.2 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365085B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-41cc8ada101e46c7b068c29a0980766b |
| Source note | uspto-grants-2008_04 |