HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-(trifluoromethyl)benzaldehyde → HCID 86760660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-(trifluoromethyl)benzaldehyde | HCID 2736672 | — |
| Reactant | 2-Morpholin-4-yl-2-phenylethylamine | HCID 3158583 | — |
| Reactant | HCID 66939902 | HCID 66939902 | — |
| Reactant | HCID 86760661 | HCID 86760661 | — |
| Product | HCID 86760660 | HCID 86760660 | — |
Reaction Steps
Following the procedure (preparation of rac-±-(2-chloro-3-trifluoromethyl-benzyl)-(trifluoro-phenyl-propyl)-amine) of Example 64, step (a) except rac-±-2-Morpholin4-yl-2-phenyl-ethylamine was used in step (a) instead of 2-chloro-3-(α,α,α-trifluoromethyl)benzylamine, and 2-chloro-3-trifluoromethyl benzaldehyde was used instead of (α,α,α-trifluoromethylphenylacetaldehyde, the title compound was sythesized as an oil, 0.27 g (88%); MS (ESI) 399 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365085B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-4d31f85e8a0f46eab7e672e78c92aef0 |
| Source note | uspto-grants-2008_04 |