HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67056716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 59677040 | HCID 59677040 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67056716 | HCID 67056716 | — |
Reaction Steps
The compound (367 mg) obtained in Example 237 was dissolved in methylene chloride (10 ml), and trifluoroacetic acid (10 ml) was added to stir the mixture at room temperature for 2 hours. The reaction mixture was dried to solid under reduced pressure. The title compound was obtained from the thus-obtained crude product and formalin in a similar manner to the process described in Example 18.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07365205B2 |
| Source dataset | uspto-grants-2008_04 |
| ORD ID | ord-0cf1445f16304161b1e13425cf71c2c2 |
| Source note | uspto-grants-2008_04 |