Benzoyl isothiocyanate → HCID 12763851, compound

HRID 903048Notes

Reaction equation

HRID 903048 reaction equation
[CH3:1][N:2]1[C:6]([NH2:7])=[CH:5][C:4]([CH3:8])=[N:3]1.C([N:17]=[C:18]=[S:19])(=O)C1C=CC=CC=1>>[CH3:1][N:2]1[C:6]([NH:7][C:18]([NH2:17])=[S:19])=[CH:5][C:4]([CH3:8])=[N:3]1

Participants

3

Reactant 2

HCID 68284Benzoyl isothiocyanateHCID 5207211,3-Dimethyl-1H-pyrazol-5-amine

Product 1

HCID 12763851HCID 12763851, compound

Procedure

1,3-Dimethyl-5-amino pyrazole (111.0 g.) and benzoyl iso thiocyanate (180.0 g.) were reacted as described in Example IV to give 110.3 g. of the product, mp 221°-224° C.

Workup

  1. customto give 110.3 g

Sources & evidence

ORD record
ord-7931d7c30c444ee8a1f657c7501ec88c
Source dataset
uspto-grants-1980_10
Patent number
US04226773

Reaction notes

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