HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178485194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 54384993 | HCID 54384993 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178485194 | HCID 178485194 | — |
Reaction Steps
Reaction of 0.5 g of 7-chloro-5-(2-fluorophenyl)-N-methoxy-α-nitro-3H-1,4-benzodiazepine-2-methanimine with methylamine in ethanol (20% v/v) gave the same workup and purification procedure colorless product, crystallized from ether/hexane; mp 140°-142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226768 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-49293084aa2146df9df01bf4351e6b09 |
| Source note | uspto-grants-1980_10 |