HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 13420165, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 2-(3-Azetidinyloxy)benzamide | HCID 12812503 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13420165 | HCID 13420165 | — |
Reaction Steps
To 8.0 g. (0.028 mole) of 2-(3-azetidinyloxy)benzamide stirring in 100 ml of dry benzene was added dropwise 1.6 g. (0.028 mole) of methylisocyanate with ice bath cooling. Stirring was continued at room temperature for 24 hours. The solid material was filtered and was recrystallized from 95% ethanol. The product (4.0 g., 57%) melted at 236°-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226861 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-6d0056a1cc0b48f8a42b21a73091dcc3 |
| Source note | uspto-grants-1980_10 |