HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 13420167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 3-[2-(Trifluoromethyl)phenoxy]azetidine | HCID 12812505 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13420167 | HCID 13420167 | — |
Reaction Steps
To a stirring solution of 3-(2-trifluoromethylphenoxy) azetidine (4.5 g., 0.02 mole) in 50 ml. of dry benzene was added slowly at room temperature 1.2 g. (0.02 mole) of methylisocyanate. After an additional 30 minutes a solid separated which was collected and recrystallized from benzene. The product (3.5 g., 68%) melted at 134°-136° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226861 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-6ab3cd699c274f039b258f156f05e8aa |
| Source note | uspto-grants-1980_10 |