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HRID903190

反应详情

EQUATION

反应方程式

HRID 903190 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Cl
HCID6367

Acetyl chloride

C2H3ClO

结构：CCOP(=O)(CN1C(=O)C(N=[N+]=[N-])C1S(C)(=O)=O)OCCC(=O)OCc1ccccc1
HCID86737251

未命名化合物

PRODUCTS

生成物

1
结构：CCOP(=O)(CN1C(=O)C(N=[N+]=[N-])C1Cl)OCCC(=O)OCc1ccccc1
HCID86737253

未命名化合物

PROCEDURE

实验过程

1-(Benzyloxycarbonyldiethylphosphono)methyl-3-azido-4-methylsulfonyl-2-azetidinone (0.446 g.) is dissolved in acetyl chloride (5 ml.). The mixture is allowed to stand for 10 minutes and the acetyl chloride is removed under reduced pressured to afford 1-(benzyloxycarbonyldiethylphosphono)methyl-3-azido-4-chloro-2-azetidinone.

WORKUP

后处理

  1. customthe acetyl chloride is removed