참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Cyanuric chloride | HCID 7954 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 2,4-Dichloro-6-(dimethylamino)-1,3,5-triazine | HCID 16985 | — |
반응 단계
A suspension of cyanuric chloride (27.6 g.) in anhydrous ether (600 ml.) was kept at -30° C. and treated with dimethylamine (13.5 g.). Following the addition the mixture was allowed to warm to 0° C. and poured on to ice. The ether layer was separated, dried, kand evaporated and the residue crystallised from light petroleum to give the product (26.0 g.) having a melting point of 123°-124° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04226990 |
|---|
| 출처 데이터셋 | uspto-grants-1980_10 |
|---|
| ORD ID | ord-268bf0d197194a8f95d104798829cfe2 |
|---|
| 출처 메모 | uspto-grants-1980_10 |
|---|
