反应详情

温度

0 °C

A suspension of cyanuric chloride (27.6 g.) in anhydrous ether (600 ml.) was kept at -30° C. and treated with dimethylamine (13.5 g.). Following the addition the mixture was allowed to warm to 0° C. and poured on to ice. The ether layer was separated, dried, kand evaporated and the residue crystallised from light petroleum to give the product (26.0 g.) having a melting point of 123°-124° C.

1. customwas kept at -30° C.
2. additionthe addition the mixture
3. additionpoured on to ice
4. customThe ether layer was separated
5. customdried
6. customevaporated
7. customthe residue crystallised from light petroleum
8. customto give the product (26.0 g.)