HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → Ethyl 3-(5,6-dimethyl-3-pyridyl)-2-formylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 3-(5,6-dimethyl-3-pyridyl)propionate | HCID 14576944 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | Ethyl 3-(5,6-dimethyl-3-pyridyl)-2-formylpropionate | HCID 12783847 | — |
Reaction Steps
Reaction of ethyl 3-(5,6-dimethyl-3-pyridyl)-propionate with ethyl formate and sodium hydride in dimethoxyethane at room temperature gave ethyl 3-(5,6-dimethyl-3-pyridyl)-2-formylpropionate, m.p. 148°-9°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04227000 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-facfd15b8eb94cdf940ed000bded43fe |
| Source note | uspto-grants-1980_10 |