HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(6-methoxy-3-pyridyl)acrylate → Ethyl 3-(6-methoxy-3-pyridyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(6-methoxy-3-pyridyl)acrylate | HCID 53930754 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(6-methoxy-3-pyridyl)propionate | HCID 12799555 | 100.2% |
Reaction Steps
Ethyl 3-(6-methoxy-3-pyridyl)acrylate (32.33 g), in ethanol (160 ml) was hydrogenated at 344 kPa at 40° using palladium-on-charcoal catalyst (5%, 0.2 g). The mixture was filtered and the filtrate was evaporated to give ethyl 3-(6-methoxy-3-pyridyl)propionate (32.7 g), as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04227000 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-c247b65dfb02443dbfc9dede9485e4e9 |
| Source note | uspto-grants-1980_10 |