HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(5,6-Dimethyl-3-pyridylmethyl)-2-nitroamino4-pyrimidone → HCID 13060036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(5,6-Dimethyl-3-pyridylmethyl)-2-nitroamino4-pyrimidone | HCID 12783831 | — |
| Reactant | 2-{[(3-Bromopyridin-2-yl)methyl]sulfanyl}ethan-1-amine | HCID 12951527 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13060036 | HCID 13060036 | — |
Reaction Steps
A mixture of 5-(5,6-dimethyl-3-pyridylmethyl)-2-nitroamino-4-pyrimidone and 1.2 molar equivalents of 2-(3-bromo-2-pyridylmethylthio)ethylamine was heated under reflux in ethanol for 48 hours, evaporated to dryness and the product isolated as 2-[2-(3-bromo-2-pyridylmethylthio)ethylamino]-5-(5,6-dimethyl-3-pyridylmethyl)-4-pyrimidone, m.p. 105°-7°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04227000 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-158be557d4d645f88d8671721789409e |
| Source note | uspto-grants-1980_10 |