HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Proline → HCID 54491809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Proline | HCID 145742 | — |
| Reactant | HCID 23337572 | HCID 23337572 | — |
| Reactant | Potassium ethanethioate | HCID 23670855 | — |
| Reactant | HCID 70526367 | HCID 70526367 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 54491809 | HCID 54491809 | — |
Reaction Steps
The preceding compound is converted to 3-(4-chloro-3-trifluoromethylbenzoyl)propionic acid, hydroxysuccinimide ester and coupled to L-proline as in Example 16. The 1-([3-(4-chloro-3-trifluoromethylbenzoyl)propionyl]-L-proline is brominated as in Example 20 and the product reacted with potassium thioacetate in ethanol-water (1:1) as in Example 21 to give the product of the Example as a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04226775 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-64b89ead6b534d6dba270a4ad91de205 |
| Source note | uspto-grants-1980_10 |