Peracetic Acid → HCID 86737265, compound

HRID 903488Notes

Reaction equation

HRID 903488 reaction equation
[C:1]([N:5]=[N:6][C:7]([O:10][CH3:11])([CH3:9])[CH3:8])([CH3:4])([CH3:3])[CH3:2].C(OO)(=[O:14])C>C(OCC)(=O)C>[C:1]([N+:5](=[N:6][C:7]([O:10][CH3:11])([CH3:9])[CH3:8])[O-:14])([CH3:4])([CH3:3])[CH3:2]

Participants

4

Reactant 2

HCID 6585Peracetic AcidHCID 23336091HCID 23336091, compound

Product 1

HCID 86737265HCID 86737265, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

2-t-Butylazoxy-2-methoxypropane was prepared by oxidizing 7.9 grams (0.05 moles) 2-t-butylazo-2-methoxypropane with 50 ml. of 25% peracetic acid in ethyl acetate at 30°-40° C. for 2 hours. The yield was 7.3 grams (84% yield) of a colorless liquid. The infrared spectrum of the product was in agreement with the structure of 2-t-butylazoxy-2-methoxypropane (2 strong bands at 1450-1510 cm-1).

Sources & evidence

ORD record
ord-d9257e02b8dd4a46aa98d6119f0b8728
Source dataset
uspto-grants-1980_10
Patent number
US04228069

Reaction notes

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