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HRID903534

反应详情

EQUATION

反应方程式

HRID 903534 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(N)=O
HCID11737

1,1-Dimethylurea

C3H8N2O

结构：OC[P+](CO)(CO)CO.[Cl-]
HCID31298

Tetramethylolphosphonium chloride

C4H12ClO4P

PRODUCTS

生成物

1
结构：CN(C)C(=O)NC[P+](CNC(=O)N(C)C)(CNC(=O)N(C)C)CNC(=O)N(C)C.[Cl-]
HCID131711912

未命名化合物

收率 99.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

Reaction of THPC (9.53 g, 0.05 mol) with 1,1-dimethylurea (17.62 g, 0.2 mol) in toluene (75 ml), following Example 1, gave 23.47 g (99.7%) of tetrakis(3,3-dimethylureidomethyl)phosphonium chloride (I, R=H, R'=R"=CH3, X=Cl) as a colorless, hygroscopic resin.