HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylurea → HCID 131711912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylurea | HCID 11737 | — |
| Reactant | Tetrakis(hydroxymethyl)phosphonium chloride | HCID 31298 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 131711912 | HCID 131711912 | 99.7% |
Reaction Steps
Reaction of THPC (9.53 g, 0.05 mol) with 1,1-dimethylurea (17.62 g, 0.2 mol) in toluene (75 ml), following Example 1, gave 23.47 g (99.7%) of tetrakis(3,3-dimethylureidomethyl)phosphonium chloride (I, R=H, R'=R"=CH3, X=Cl) as a colorless, hygroscopic resin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04228100 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-3422916d40234d928bbc06e7550c8b4f |
| Source note | uspto-grants-1980_10 |