Urea → HCID 86735370, compound

HRID 903542Notes

Reaction equation

HRID 903542 reaction equation
[CH2:1]([P+:3]([CH2:8][OH:9])([CH2:6][OH:7])[CH2:4][OH:5])[OH:2].[CH2:10]([P+:12]([CH2:17][OH:18])([CH2:15][OH:16])[CH2:13][OH:14])[OH:11].[O-:19][S:20]([O-:23])(=[O:22])=[O:21].[NH2:24][C:25]([NH2:27])=[O:26].CCC(COC(C(N(CC[NH+](C)C)C)=O)(C1C=CC=CC=1)C1C=CC=CC=1)CC.[Cl-]>O>[NH2:24][C:25]([NH2:27])=[O:26].[CH2:1]([P+:3]([CH2:8][OH:9])([CH2:6][OH:7])[CH2:4][OH:5])[OH:2].[CH2:10]([P+:12]([CH2:17][OH:18])([CH2:15][OH:16])[CH2:13][OH:14])[OH:11].[O-:22][S:20]([O-:23])(=[O:21])=[O:19]

Participants

5

Reactant 3

HCID 1176UreaHCID 19153X 100HCID 41478Tetrakis(hydroxymethyl)phosphonium sulfate

Product 1

HCID 86735370HCID 86735370, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A urea/THPS formulation was prepared by mixing 75% THPS (43.68 g, 80.6 mmol) with urea (19.36 g, 322.4 mmol) and Triton X-100 (0.1 g), and making up to 100 g with water. The formulation was applied to desized, scoured, and bleached 80×80 cotton printcloth to a 100-110% wet pickup, cured at 100° C. in a forced draft oven for the time indicated, rinsed in hot running tap water for 15 min, and line dried. The results are given in Table VI.

Workup

  1. customcured at 100° C. in a forced draft oven for the time
  2. washrinsed
  3. customfor 15 min
  4. customline dried

Sources & evidence

ORD record
ord-4771b517b48b48cf8d7e472a19c0241a
Source dataset
uspto-grants-1980_10
Patent number
US04228100

Reaction notes

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