Sodium Bicarbonate → HCID 23336682, compound

HRID 903578Notes

Reaction equation

HRID 903578 reaction equation
[O:1]=[C:2]1[C:7]2[CH:8]=[C:9]3[C:18](=[O:19])[CH:17]=[C:16]([C:20]([OH:22])=[O:21])[S:15][C:10]3=[C:11]([CH2:12][CH2:13][CH3:14])[C:6]=2[O:5][C:4]([C:23]([OH:25])=[O:24])=[CH:3]1.C(=O)(O)[O-].[Na+:30]>O>[O:1]=[C:2]1[C:7]2[CH:8]=[C:9]3[C:18](=[O:19])[CH:17]=[C:16]([C:20]([O-:22])=[O:21])[S:15][C:10]3=[C:11]([CH2:12][CH2:13][CH3:14])[C:6]=2[O:5][C:4]([C:23]([O-:25])=[O:24])=[CH:3]1.[Na+:30].[Na+:30]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 23336676HCID 23336676, compound

Product 1

HCID 23336682HCID 23336682, compoundYield 101.3%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The product of step (h) (1.935 g) and sodium bicarbonate (0.903 g) in distilled water (50 mls) were shaken until complete dissolution had occurred. The solution was filtered and the filtrate freeze dried to give 2.2 g of the desired product.

Workup

  1. filtrationThe solution was filtered
  2. customthe filtrate freeze dried

Sources & evidence

ORD record
ord-0ea4acd0a04246ca8d7c7d38d5b87595
Source dataset
uspto-grants-1980_10
Patent number
US04228173

Reaction notes

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