HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 45586, compound → HCID 23336469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 45586 | HCID 45586 | — |
| Reactant | Methyl 4-chloroformylbutyrate | HCID 73916 | — |
| Product | HCID 23336469 | HCID 23336469 | 73.5% |
Reaction Steps
10 g of N-isobutyl-tryptamine (i.e., 3-(2-isobutylaminoethyl)-indole) and 9.1 g of 4-methoxycarbonylbutyryl chloride were treated in the same manner as described in Example 1. 11.23 g of N-isobutyl-N-(4-methoxycarbonylbutyl)-tryptamine (i.e., 3-[2-(N-isobutyl-4-methoxycarbonylbutanamido)ethyl]-indole) were thereby obtained. Yield: 70.5%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04228168 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-f4874ceb878344fa8a4ce3824dd947b3 |
| Source note | uspto-grants-1980_10 |