HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 70586823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 57212445 | HCID 57212445 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70586823 | HCID 70586823 | — |
Reaction Steps
Equimolar quantities of 17-cyclopropylmethyl-3,14β-dihydroxy-6-oxamorphinan (XVI), acetyl chloride and pyridine are mixed together in dry methylene chloride and the resultant mixture is heated at reflux for several hours to produce the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04228285 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-d89301602678468abc6235a1dd6a76b9 |
| Source note | uspto-grants-1980_10 |