HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 23335098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Carbamoyl-1,2-phenylene diacetate | HCID 13364121 | — |
| Reactant | HCID 18955474 | HCID 18955474 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23335098 | HCID 23335098 | — |
Reaction Steps
The procedure used in Example 1 (1) was repeated except that 3,4,5-triacetoxybenzamide (8.0 g) and oxalyl chloride (8.6 g) were used instead of 3,4-diacetoxybenzamide (7.5 g) and oxalyl chloride (10.1 g) to give a solution of 3,4,5-triacetoxybenzoyl isocyanate in anhydrous dichloromethane (40 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04229348 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-f8c9fcab15644f99acb2efe26fa39dfe |
| Source note | uspto-grants-1980_10 |