Oxalyl chloride → HCID 23335098, compound

HRID 903808Notes

Reaction equation

HRID 903808 reaction equation
[C:1]([O:4][C:5]1[CH:6]=[C:7]([CH:11]=[C:12]([O:18][C:19](=[O:21])[CH3:20])[C:13]=1[O:14][C:15](=[O:17])[CH3:16])[C:8]([NH2:10])=[O:9])(=[O:3])[CH3:2].C(Cl)(=O)[C:23](Cl)=[O:24].C(OC1C=C(C=CC=1OC(=O)C)C(N)=O)(=O)C>ClCCl>[C:1]([O:4][C:5]1[CH:6]=[C:7]([CH:11]=[C:12]([O:18][C:19](=[O:21])[CH3:20])[C:13]=1[O:14][C:15](=[O:17])[CH3:16])[C:8]([N:10]=[C:23]=[O:24])=[O:9])(=[O:3])[CH3:2]

Participants

5

Reactant 3

HCID 65578Oxalyl chloride2×HCID 133641214-Carbamoyl-1,2-phenylene diacetateHCID 18955474HCID 18955474, compound

Product 1

HCID 23335098HCID 23335098, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The procedure used in Example 1 (1) was repeated except that 3,4,5-triacetoxybenzamide (8.0 g) and oxalyl chloride (8.6 g) were used instead of 3,4-diacetoxybenzamide (7.5 g) and oxalyl chloride (10.1 g) to give a solution of 3,4,5-triacetoxybenzoyl isocyanate in anhydrous dichloromethane (40 ml).

Sources & evidence

ORD record
ord-f8c9fcab15644f99acb2efe26fa39dfe
Source dataset
uspto-grants-1980_10
Patent number
US04229348

Reaction notes

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