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HRID903839

反应详情

EQUATION

反应方程式

HRID 903839 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(N)c(Cl)c1.O=S(=O)(O)O
HCID22584

2-Chloro-1,4-diaminobenzene sulfate (1:1)

C6H9ClN2O4S

结构：CCOP(=O)(N=C=S)OCC
HCID556832

1-[ethoxy(isothiocyanato)phosphoryl]oxyethane

C5H10NO3PS

PRODUCTS

生成物

1
结构：CCOP(=O)(NC(=S)Nc1ccc(NC(=S)NP(=O)(OCC)OCC)c(Cl)c1)OCC
HCID131711916

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

Employing the process of Example 1 in every detail except that 2-chloro-p-phenylenediamine sulfate is neutralized and allowed to react with two equivalents of diethyl phosphoroisothiocyanatidate ##STR7## in chloroform instead of methylene chloride to afford the title compound, m.p. 148°-149° C.