HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dichloroethane → HCID 23335648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dichloroethane | HCID 6365 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | N-(2-hydroxypropyl)methacrylamide | HCID 38622 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 23335648 | HCID 23335648 | — |
Reaction Steps
The compound was prepared by the method described in Example 7, using N-(2-hydroxypropyl)methacrylamide (14.3 g), dichloroethane (200 ml), chloroacetyl chloride (11.3 g) and triethylamine (10.1 g). The product distilled at 112° C./0.1 mm (12 g) and was obtained as a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04229519 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-27e5d3f37b294181ab27e7252c91f95d |
| Source note | uspto-grants-1980_10 |