1,1-Dichloroethane → HCID 23335648, compound

HRID 903984Notes

Reaction equation

HRID 903984 reaction equation
[OH:1][CH:2]([CH3:10])[CH2:3][NH:4][C:5](=[O:9])[C:6]([CH3:8])=[CH2:7].ClC(Cl)C.[Cl:15][CH2:16][C:17](Cl)=[O:18]>C(N(CC)CC)C>[Cl:15][CH2:16][C:17]([O:1][CH:2]([CH3:10])[CH2:3][NH:4][C:5](=[O:9])[C:6]([CH3:8])=[CH2:7])=[O:18]

Participants

5

Reactant 3

HCID 63651,1-DichloroethaneHCID 6577Chloroacetyl chlorideHCID 38622N-(2-hydroxypropyl)methacrylamide

Product 1

HCID 23335648HCID 23335648, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The compound was prepared by the method described in Example 7, using N-(2-hydroxypropyl)methacrylamide (14.3 g), dichloroethane (200 ml), chloroacetyl chloride (11.3 g) and triethylamine (10.1 g). The product distilled at 112° C./0.1 mm (12 g) and was obtained as a viscous oil.

Workup

  1. customThe compound was prepared by the method
  2. distillationThe product distilled at 112° C./0.1 mm (12 g)
  3. customwas obtained as a viscous oil

Sources & evidence

ORD record
ord-27e5d3f37b294181ab27e7252c91f95d
Source dataset
uspto-grants-1980_10
Patent number
US04229519

Reaction notes

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