HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Methylphenyl propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Propionyl chloride | HCID 62324 | — |
| Product | 2-Methylphenyl propanoate | HCID 221436 | 98% |
Reaction Steps
Into a spherical flask equipped with a condenser, a dropping funnel and containing 2 mols of o-cresol are introduced, in 15 minutes, 2.2 mols of propionyl chloride. The mixture as obtained is heated at 110° C. for about 2 hours, until the discharge of hydrochloric acid ceases. The o-cresol propionate which is obtained is distilled under vacuum:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230624 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-369d4ee0ac27406580cadfc6b43d5bbf |
| Source note | uspto-grants-1980_10 |