HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Acetic acid, 2-methylphenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Product | Acetic acid, 2-methylphenyl ester | HCID 10778 | 95% |
Reaction Steps
Into a spherical flask provided with a condenser, a dropping funnel and containing 2 moles of o-cresol, 2.4 moles of acetyl chloride are introduced in 15 minutes. The bath is kept at 110° C. until the release of hydrochloric acid is completed, i.e. after about 3 hours, and then the o-cresol acetate as obtained is distilled under vacuum:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230624 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-5d24bdc1bbd34a8786535ebdd5d69f9c |
| Source note | uspto-grants-1980_10 |