HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 23333511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 54083180 | HCID 54083180 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 23333511 | HCID 23333511 | — |
Reaction Steps
To 4.54 g (15 mmole) 4-(hexafluoro-2-hydroxy-2-propyl)-2-methoxy-6-methylaniline in 25 ml pyridine, add 1.94 g (17 mmole) methanesulfonyl chloride. After 16 hours, pour onto 200 ml H2O and filter the solid. Recrystallize from Et2O-hexane to obtain the product; m.p. 109°-110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230635 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-880adc1264a048aea6edf25b1a74d732 |
| Source note | uspto-grants-1980_10 |