HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 23333614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 23333586 | HCID 23333586 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23333614 | HCID 23333614 | 79.4% |
Reaction Steps
A mixed liquid of methyl 5,6-dihydro-5-n-propyl-11-oxodibenz[b,e]azepine-2-acetate (0.5 g), sodium hydroxide (2 g), methanol (20 ml) and water (10 ml) was treated in the same manner as described in Example 21 to afford the desired compound (0.38 g) as yellow powdery crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230703 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-3ec09ce6beae47b7b08d22ff54d225d3 |
| Source note | uspto-grants-1980_10 |