HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 23333627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 21814004 | HCID 21814004 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23333627 | HCID 23333627 | 14.6% |
Reaction Steps
5,6-Dihydro-5-benzyl-11-oxodibenz[b,e]azepine (6.2 g), anhydrous aluminum chloride (6.07 g), acetyl chloride (4.87 g) and methylene chloride (60 ml) were treated in the same manner as described in Example 25 to obtain the desired compound (1.03 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230703 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-ac786e08985b4542a6973fb3ed29c766 |
| Source note | uspto-grants-1980_10 |