HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(15-Carboxypentadecylamino)benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(15-Carbomethoxypentadecylamino)benzonitrile | HCID 21163376 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-(15-Carboxypentadecylamino)benzonitrile | HCID 21163363 | — |
Reaction Steps
A solution of 3 g. of 4-(15-carbomethoxypentadecylamino)benzonitrile and 0.5 g. of potassium hydroxide in 50 ml. of 95% ethanol is stirred at 50° C. for 10 hours, diluted with water and acidified with dilute hydrochloric acid. The precipitate is collected, dried and recrystallized from ether-hexane to yield 4-(15-carboxypentadecylamino)benzonitrile as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230628 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-1fef47bf7d7c45e9b32c210980f0d9a9 |
| Source note | uspto-grants-1980_10 |