HRID904286

反应详情

EQUATION

反应方程式

HRID 904286 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

To 200 g of malic acid was added 175 cc of concentrated sulfuric acid and 1 g of 65% oleum. The mixture was heated to 100° C. for two hours, cooled to 30° C. and diluted with 300 cc of water. The reaction mixture was cooled to 25° C. and filtered to give coumalic acid.

WORKUP

后处理

  1. temperaturecooled to 30° C.
  2. temperatureThe reaction mixture was cooled to 25° C.
  3. filtrationfiltered