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HRID904291

反应详情

EQUATION

反应方程式

HRID 904291 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCCCl.Cl
HCID94308

Dimethylaminopropyl chloride hydrochloride

C5H13Cl2N

结构：O=c1oc2ccccc2c(O)c1-c1ccccc1
HCID54688870

Coumarin, 4-hydroxy-3-phenyl-

C15H10O3

PRODUCTS

生成物

1
结构：CN(C)CCCOc1c(-c2ccccc2)c(=O)oc2ccccc12
HCID23334031

未命名化合物

收率 59%

PROCEDURE

实验过程

By treating 10 g. (0.042 mol) of 3-phenyl-4-hydroxy-coumarin with 87 g. (0.055 mol) of 3-dimethylamino-1-chloropropane hydrochloride as described in Example 1, there are obtained 8.1 g. of a yellow oil which cannot be crystallised. Yield 59% (theoretical yield 13.6 g.).

WORKUP

后处理

  1. additionBy treating 10 g
  2. customare obtained 8.1 g
  3. customof a yellow oil which cannot be crystallised