HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Chloroethyl)morpholine → HCID 23334087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Chloroethyl)morpholine | HCID 76727 | — |
| Reactant | 3-Butyl-4,5,7-trihydroxy-2H-1-benzopyran-2-one | HCID 54721337 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23334087 | HCID 23334087 | 45% |
Reaction Steps
7.5 g. (0.03 mol) of 3-butyl-4,5,7-trihydroxy-coumarin are treated with 17.5 g. (0.117 mol) of 2-morpholino-1-chlorethane, as in Example 1. A beige-coloured solid is obtained. M.P. 131° C. (ethanol). Weight 7.7 g.; yield 45% (theoretical yield 17.7 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-1ff4d327cff146cf80713ad1db98a568 |
| Source note | uspto-grants-1980_10 |