HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22226923, compound → HCID 23334097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22226923 | HCID 22226923 | — |
| Reactant | 4-Hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin | HCID 54721330 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23334097 | HCID 23334097 | 71% |
Reaction Steps
The desired product is prepared according to the method of Example 9 from 14.5 g. (0.06 mol) of 3-phenyl-4-hydroxy-5,6,7,8-tetrahydro-coumarin and 11.7 g. (0.078 mol) of 2-morpholino-2-chlorethane. M.P. 115° C. (ethanol); weight 15.1 g. (yield 71%, theoretical yield 21.3 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-a4d53b15820e4a67b8403dc379a39407 |
| Source note | uspto-grants-1980_10 |