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HRID904299

反应详情

EQUATION

反应方程式

HRID 904299 的结构方程式

REACTANTS

反应物

2
结构：CC(CCl)CN1CCOCC1.Cl
HCID23334092

未命名化合物

结构：O=c1oc2ccccc2c(O)c1-c1ccccc1
HCID54688870

Coumarin, 4-hydroxy-3-phenyl-

C15H10O3

PRODUCTS

生成物

1
结构：CC(COc1c(-c2ccccc2)c(=O)oc2ccccc12)CN1CCOCC1
HCID23334099

未命名化合物

收率 82.5%

PROCEDURE

实验过程

This compound is prepared according to the method of Example 8 from 14.3 g. (0.06 mol) of 4-hydroxy-3-phenyl-coumarin and 16.7 g. (0.078 mol) of 3-morpholino-2-methyl-1-chloropropane hydrochloride. After recrystallisation from ethanol, 18.8 g. are obtained. Yield 82.5% (theoretical yield 22.8 g.); M.P. 113° C.

WORKUP

后处理

  1. customThis compound is prepared
  2. customAfter recrystallisation from ethanol, 18.8 g
  3. customare obtained