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HRID904302

反应详情

EQUATION

反应方程式

HRID 904302 的结构方程式

REACTANTS

反应物

2
结构：ClCCN1CCOCC1
HCID76727

Morpholine, 4-(2-chloroethyl)-

C6H12ClNO

结构：COc1ccc2oc(=O)c(-c3ccccc3)c(O)c2c1
HCID54705896

4-Hydroxy-6-methoxy-3-phenyl-2H-1-benzopyran-2-one

C16H12O4

PRODUCTS

生成物

1
结构：COc1ccc2oc(=O)c(-c3ccccc3)c(OCCN3CCOCC3)c2c1
HCID23334084

未命名化合物

收率 67.5%

PROCEDURE

实验过程

This compound is obtained according to the method of Example 8 from 12.1 g. (0.045 mol) of 6-methoxy-3-phenyl-4-hydroxy-coumarin and 10.9 g. (0.057 mol) of 2-morpholino-1-chlorethane. After recrystallisation from isopropanol, 11.3 g. of a beige-coloured solid are obtained. M.P. 118° C.; yield 67.5% (theoretical yield 16.7 g.).

WORKUP

后处理

  1. customThis compound is obtained
  2. customAfter recrystallisation from isopropanol, 11.3 g
  3. customof a beige-coloured solid are obtained