HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Chloroethyl)morpholine → HCID 23334083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Chloroethyl)morpholine | HCID 76727 | — |
| Reactant | HCID 54690405 | HCID 54690405 | — |
| Product | HCID 23334083 | HCID 23334083 | 82.5% |
Reaction Steps
Obtained according to the method of Example 8, from 12.1 g. (0.045 mol) of 3-(4'-methoxyphenyl)-4-hydroxy-coumarin and 8.7 g. (0.058 mol) of 2-morpholino-1-chlorethane. After recrystallisation from ethanol, there are obtained 14.7 g. of a beige product; M.P. 104° C. Yield 82.5% (theoretical yield 17.1 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-f6e12b9afbd94aec806cdacb724386ae |
| Source note | uspto-grants-1980_10 |