HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylaminoethyl chloride → HCID 23334096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylaminoethyl chloride | HCID 13364 | — |
| Reactant | 4-Hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin | HCID 54721330 | — |
| Product | HCID 23334096 | HCID 23334096 | 68.7% |
Reaction Steps
Prepared as indicated in Example 14, Stage B, from 12.1 g. (0.05 mol) of 4-hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin (Example 14, Stage A) and 8.8 g. (0.065 mol) of 2-diethylamino-1-chloroethane. 13.2 g. of an oil are obtained, which cannot be crystallised. Yield 68.7% (theoretical yield 19.2 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-d8c7577769064dc79837dfa8ce0ed708 |
| Source note | uspto-grants-1980_10 |