HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19907059, compound → HCID 23334037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19907059 | HCID 19907059 | — |
| Reactant | 4-Hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin | HCID 54721330 | — |
| Product | HCID 23334037 | HCID 23334037 | 83.5% |
Reaction Steps
Prepared as indicated in Example 14, Stage B, from 29 g. (0.12 mol) of 4-hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin and 27.3 g. (0.156 mol) of 3-morpholino-2-methyl-2-chloropropane. 38.2 g. of an oil which cannot be crystallised are obtained. Yield 83.5% (theoretical yield 45.6 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-1eb126b3a9d74bf8b8ca4b90cd39c874 |
| Source note | uspto-grants-1980_10 |