N-(3-Chloropropyl)dibutylamine → HCID 23334069, compound

HRID 904317Notes

Reaction equation

HRID 904317 reaction equation
[OH:1][C:2]1[C:11]2[CH2:10][CH2:9][CH2:8][CH2:7][C:6]=2[O:5][C:4](=[O:12])[C:3]=1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.Cl[CH2:20][CH2:21][CH2:22][N:23]([CH2:28][CH2:29][CH2:30][CH3:31])[CH2:24][CH2:25][CH2:26][CH3:27]>>[CH2:28]([N:23]([CH2:24][CH2:25][CH2:26][CH3:27])[CH2:22][CH2:21][CH2:20][O:1][C:2]1[C:11]2[CH2:10][CH2:9][CH2:8][CH2:7][C:6]=2[O:5][C:4](=[O:12])[C:3]=1[C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1)[CH2:29][CH2:30][CH3:31]

Participants

3

Reactant 2

HCID 96084N-(3-Chloropropyl)dibutylamineHCID 547213304-Hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin

Product 1

HCID 23334069HCID 23334069, compoundYield 80.5%

Procedure

As in Example 14, Stage B, 14.5 g. (0.06 mol) of 4-hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin are caused to react with 16.2 g. (0.078 mol) of 1-chloro-3-dibutylaminopropane. 19.8 g. of an oil which cannot be crystallised are obtained. Yield 80.5% (theoretical yield 24.6 g.).

Workup

  1. customto react with 16.2 g
  2. customof an oil which cannot be crystallised
  3. customare obtained

Sources & evidence

ORD record
ord-36f205f2339843bc84c1280c0f45a793
Source dataset
uspto-grants-1980_10
Patent number
US04230850

Reaction notes

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