HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-Chloropropyl)dibutylamine → HCID 23334069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-Chloropropyl)dibutylamine | HCID 96084 | — |
| Reactant | 4-Hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin | HCID 54721330 | — |
| Product | HCID 23334069 | HCID 23334069 | 80.5% |
Reaction Steps
As in Example 14, Stage B, 14.5 g. (0.06 mol) of 4-hydroxy-3-phenyl-5,6,7,8-tetrahydrocoumarin are caused to react with 16.2 g. (0.078 mol) of 1-chloro-3-dibutylaminopropane. 19.8 g. of an oil which cannot be crystallised are obtained. Yield 80.5% (theoretical yield 24.6 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-36f205f2339843bc84c1280c0f45a793 |
| Source note | uspto-grants-1980_10 |