HRID904318

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID76727

Morpholine, 4-(2-chloroethyl)-

C6H12ClNO

结构：O=c1oc2c(-c3ccccc3)cccc2c(O)c1-c1ccccc1

HCID54688869

4-Hydroxy-3,8-diphenyl-2H-chromen-2-one

C21H14O3

PRODUCTS

生成物

结构：O=c1oc2c(-c3ccccc3)cccc2c(OCCN2CCOCC2)c1-c1ccccc1

HCID23334090

未命名化合物

收率 75%

PROCEDURE

实验过程

15.7 g. (0.05 mol) of 4-hydroxy-3,8-diphenyl-coumarin are treated, as in Example 8, with 9.7 g. (0.065 mol) of 1-chloro-2-morpholinoethane. After recrystallisation from isopropanol, 16 g. are obtained. M.P. 106°-108° C. Yield 75% (theoretical yield 21.3 g.).

WORKUP

后处理

customAfter recrystallisation from isopropanol, 16 g
customare obtained