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HRID904319

反应详情

EQUATION

反应方程式

HRID 904319 的结构方程式

REACTANTS

反应物

2
结构：CC(CCl)CN1CCOCC1
HCID23334047

未命名化合物

结构：O=c1oc2c(O)cccc2c(O)c1-c1ccccc1
HCID54721333

未命名化合物

PRODUCTS

生成物

1
结构：CC(COc1c(-c2ccccc2)c(=O)oc2c(O)cccc12)CN1CCOCC1
HCID23334091

未命名化合物

收率 60.7%

PROCEDURE

实验过程

Prepared according to the method of Example 30 by alkylation of 4,8-dihydroxy-3-phenyl-coumarin by 1-chloro-2-methyl-3-morpholino-propane. After recrystallisation from isopropanol, a white solid is obtained with the melting point of 136° C. Yield 60.7%.

WORKUP

后处理

  1. customPrepared
  2. customAfter recrystallisation from isopropanol
  3. customa white solid is obtained with the melting point of 136° C